2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- → HCID 145795656, 화합물

HRID 461042

반응식

HRID 461042 반응식
[ClH:1].[C:2]1([C@H:8]2[CH2:12][CH2:11][CH2:10][C@H:9]2[NH2:13])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.COC1[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][N:22]=1.Cl.C1([C@H]2CCC[C@H]2N)CCCCC1.COC1CCCCN=1>>[ClH:1].[CH:2]1([C@H:8]2[CH2:12][CH2:11][CH2:10][C@H:9]2[N:13]=[C:21]2[CH2:20][CH2:19][CH2:18][CH2:17][NH:22]2)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

참가 물질

5

반응물 4

HCID 756572H-Azepine, 3,4,5,6-tetrahydro-7-methoxy-HCID 138567o-MethylvalerolactimHCID 70050481cis-2-Cyclohexylcyclopentylamine hydrochlorideHCID 70051154rac-(1R,2R)-2-phenylcyclopentan-1-amine hydrochloride

생성물 1

HCID 145795656HCID 145795656, 화합물

실험 절차

Following the procedure of Example 23, only substituting for cis-2-phenylcyclopentylamine hydrochloride and O-methylcaprolactim, appropriate amounts of cis-2-(cyclohexyl)cyclopentylamine hydrochloride and O-methylvalerolactim respectively the desired product is obtained, M.P. 195.5°-197° C.

출처 및 근거

ORD 기록
ord-f7e359947188445885dbe2d74e1dd436
출처 데이터셋
uspto-grants-1977_12
특허 번호
US04061746

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