Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2-Chloro-4'-methyl-3'-sulfamoylacetophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Isopropanol | HCID 3776 | — |
| 반응물 | 4'-Methyl-3'-sulfamoyl-diazoacetophenone | HCID 54047535 | — |
| 용매 | Diglyme | HCID 8150 | — |
| 생성물 | 2-Chloro-4'-methyl-3'-sulfamoylacetophenone | HCID 13628783 | — |
반응 단계
10 g of 4'-methyl-3'-sulfamoyl-diazoacetophenone were reacted as prescribed in Example 66b) in diethylene glycol dimethyl ether with 37% HCl and worked up. Colorless crystals, melting point: 166° C (from isopropanol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04061761 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-090ae4e346d942ee9c943031c6a5fdbd |
| 출처 메모 | uspto-grants-1977_12 |