N,N'-Diethylthiourea → 3-Ethyl-2-ethylimino-4-(4-isopropyl-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride

HRID 461161

반응식

HRID 461161 반응식
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH:11]([CH3:13])[CH3:12])=[C:7]([S:14](=[O:17])(=[O:16])[NH2:15])[CH:6]=1)=[O:4].[CH2:18]([NH:20][C:21]([NH:23][CH2:24][CH3:25])=[S:22])[CH3:19]>>[ClH:1].[CH2:24]([N:23]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([CH:11]([CH3:13])[CH3:12])=[C:7]([S:14](=[O:17])(=[O:16])[NH2:15])[CH:6]=2)([OH:4])[CH2:2][S:22][C:21]1=[N:20][CH2:18][CH3:19])[CH3:25]

참가 물질

3

반응물 2

HCID 2735009N,N'-DiethylthioureaHCID 227606662-Chloro-4'-isopropyl-3'-sulfamoylacetophenone

생성물 1

HCID 227606713-Ethyl-2-ethylimino-4-(4-isopropyl-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride

실험 절차

5.5 g of 2-chloro-4'isopropyl-3'-sulfamoylacetophenone and 2.2 g of 1,3-diethylthio urea were reacted and worked up as prescribed in Example 12. Colorless solid body, decomposition beginning at 96° C, γC=N 1610 cm-1.

후처리

  1. customat 96° C

출처 및 근거

ORD 기록
ord-6d66f298bf38433788dccb257f970ab9
출처 데이터셋
uspto-grants-1977_12
특허 번호
US04061761

연결된 노트

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