Iodoethane → N-Butyl-N'-(5-tert-butyl-1,2-oxazol-3-yl)-N'-ethyl-N-methylurea

HRID 461355노트

반응식

HRID 461355 반응식
[CH3:1][N:2]([CH2:15][CH2:16][CH2:17][CH3:18])[C:3]([NH:5][C:6]1[CH:10]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[O:8][N:7]=1)=[O:4].[CH2:19](I)[CH3:20]>>[CH3:1][N:2]([CH2:15][CH2:16][CH2:17][CH3:18])[C:3]([N:5]([CH2:19][CH3:20])[C:6]1[CH:10]=[C:9]([C:11]([CH3:12])([CH3:13])[CH3:14])[O:8][N:7]=1)=[O:4]

참가 물질

3

반응물 2

HCID 6340IodoethaneHCID 20534526N-Butyl-N'-(5-tert-butyl-1,2-oxazol-3-yl)-N-methylurea

생성물 1

HCID 22768148N-Butyl-N'-(5-tert-butyl-1,2-oxazol-3-yl)-N'-ethyl-N-methylurea

실험 절차

The reaction is effected as in Example 171 by using 1-methyl-1-butyl-3-(5-t-butyl-3-isoxazolyl)urea and ethyl iodide to give 1-methyl-1-butyl-3-ethyl-3-(5-t-butyl-3-isoxazolyl)urea as an oil boiling at 130° to 135° C (bath temperature)/0.25 mm Hg.

출처 및 근거

ORD 기록
ord-40decb456a4042289c7c1cb1e12989d9
출처 데이터셋
uspto-grants-1977_12
특허 번호
US04062861

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