Methyl iodide → HCID 22768153, 화합물

HRID 461356노트

반응식

HRID 461356 반응식
[CH2:1]([N:3]([CH2:16][CH2:17][CH2:18][CH3:19])[C:4]([NH:6][C:7]1[CH:11]=[C:10]([C:12]([CH3:15])([CH3:14])[CH3:13])[O:9][N:8]=1)=[O:5])[CH3:2].[CH3:20]I>>[CH2:1]([N:3]([CH2:16][CH2:17][CH2:18][CH3:19])[C:4]([N:6]([CH3:20])[C:7]1[CH:11]=[C:10]([C:12]([CH3:13])([CH3:15])[CH3:14])[O:9][N:8]=1)=[O:5])[CH3:2]

참가 물질

3

반응물 2

HCID 6328Methyl iodideHCID 22768165N-Butyl-N'-(5-tert-butyl-1,2-oxazol-3-yl)-N-ethylurea

생성물 1

HCID 22768153HCID 22768153, 화합물

실험 절차

The reaction is effected as in Example 171 by using 1-ethyl-1-butyl-3-(5-t-butyl-3-isoxazolyl)urea and methyl iodide to give 1-ethyl-1-butyl-3-methyl-3-(5-t-butyl-3-isoxazolyl)urea as an oil boiling at 140° to 145° C (bath temperature)/0.67 mm Hg.

출처 및 근거

ORD 기록
ord-6d9ecf95f6ae4d3e9c5298a9e69558d6
출처 데이터셋
uspto-grants-1977_12
특허 번호
US04062861

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