Cyclohexyl bromide → Cyclohexyldicyclohexylphosphinodithioate

HRID 461609

반응식

[CH:1]1(Br)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH:8]1([P:14]([CH:17]2[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]2)([SH:16])=[S:15])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1>>[CH:1]1([S:16][P:14]([CH:17]2[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]2)([CH:8]2[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]2)=[S:15])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

참가 물질

반응물 2

HCID 7960Cyclohexyl bromide

HCID 75641Phosphinodithioic acid, dicyclohexyl-

생성물 1

HCID 21391611Cyclohexyldicyclohexylphosphinodithioate

실험 절차

Cyclohexylbromide was reacted with the ammonium salt of dicyclohexylphosphinodithioic acid to obtain cyclohexyldicyclohexylphosphinodithioate, m.p. 82°-85° C, which on testing lasted 1250 hours* longer than the control. The average number of hours required to reach failure was 3.5 times that of the control.

출처 및 근거

ORD 기록: ord-b4436844ded644a6b23e9bb82fa7c71b
출처 데이터셋: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04064106

연결된 노트

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