Acetic Anhydride → HCID 20560054, 화합물
반응식
[NH2:1][C:2]1[CH:17]=[CH:16][CH:15]=[CH:14][C:3]=1[CH2:4][CH2:5][C:6]1[CH:11]=[CH:10][C:9]([CH2:12][CH3:13])=[CH:8][N:7]=1.[C:18](OC(=O)C)(=[O:20])C.NC1C=CC=CC=1CCC1C=CC=CN=1>C(O)=O>[CH2:12]([C:9]1[CH:10]=[CH:11][C:6]([CH2:5][CH2:4][C:3]2[CH:14]=[CH:15][CH:16]=[CH:17][C:2]=2[NH:1][CH:18]=[O:20])=[N:7][CH:8]=1)[CH3:13]참가 물질
5
실험 절차
Reaction of 2-(o-aminophenethyl)-5-ethylpyridine with acetic anhydride and formic acid according to the procedure described in Example 2 (b) for 2-(o-aminophenethyl)pyridine provides the formylated product 5-ethyl-2-(o-formamidophenethyl)pyridine which can be crystallized from isopropyl ether, m.p. 62°-63.5° C. (corr.).
출처 및 근거
- ORD 기록
- ord-7aae3238e3274839b41ea09233469e79
- 출처 데이터셋
- uspto-grants-1977_12
- 특허 번호
- US04064254
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