3,4-Dichlorobenzenethiol → 7-[4-(3,4-Dichloro-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463196노트

반응식

HRID 463196 반응식
CS(O[CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]1[CH:23]=[CH:22][C:14]2[C:15]([CH3:21])([CH3:20])[O:16][C:17](=[O:19])[NH:18][C:13]=2[CH:12]=1)(=O)=O.[Cl:24][C:25]1[CH:26]=[C:27]([SH:32])[CH:28]=[CH:29][C:30]=1[Cl:31]>>[Cl:24][C:25]1[CH:26]=[C:27]([S:32][CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]2[CH:23]=[CH:22][C:14]3[C:15]([CH3:20])([CH3:21])[O:16][C:17](=[O:19])[NH:18][C:13]=3[CH:12]=2)[CH:28]=[CH:29][C:30]=1[Cl:31]

참가 물질

3

반응물 2

HCID 799643,4-DichlorobenzenethiolHCID 20281668HCID 20281668, 화합물

생성물 1

HCID 202817297-[4-(3,4-Dichloro-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

실험 절차

Prepared analogously to Example 210 from 7-(4-methanesulfonyloxy-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 3,4-dichloro-thiophenol.

출처 및 근거

ORD 기록
ord-5cab1b5fb431451aa26c98a546ac4ce0
출처 데이터셋
uspto-grants-1985_05
특허 번호
US04518597

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