Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Butanol → HCID 178454803, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Butanol | HCID 263 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | HCID 178476830 | HCID 178476830 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | HCID 178454803 | HCID 178454803 | 81.6% |
반응 단계
A solution of α-hydroxyethylphosphinic acid (2.2 g) and 1-butanol (5.0 g) in benzene (30 ml) was heated for 3 hours with removal of water through a Dean-Stark apparatus. After cooling, the reaction mixture was washed with water, dried over magnesium sulfate and concentrated in vacuo to give 2.71 g (81.6%) of n-butyl α-hydroxyethylphosphinate (Compound No. 5).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04544652 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-1d8432d027704c71b7d7c4dea8657e9c |
| 출처 메모 | uspto-grants-1985_10 |