Methyl iodide → Methyl 4-chlorobenzene-1-carboximidothioate hydroiodide

HRID 463883노트

반응식

HRID 463883 반응식
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[S:7])=[CH:4][CH:3]=1.[CH3:11][I:12]>CC(C)=O>[IH:12].[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([S:7][CH3:11])=[NH:8])=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 27348264-Chlorothiobenzamide

생성물 1

HCID 2777317Methyl 4-chlorobenzene-1-carboximidothioate hydroiodide

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A 17.16 g portion of 4-chlorothiobenzamide was dissolved in 80 ml of acetone and 15.14 g of methyl iodide was added. The mixture was stirred for 2 hours and then the solid was collected, washed with acetone and dried, giving 21.3 g of 4-chlorobenzenecarboximidothioic acid, methyl ester, hydroiodide.

후처리

  1. customthe solid was collected
  2. washwashed with acetone
  3. customdried

출처 및 근거

ORD 기록
ord-1ede6d8960aa44a1ae0763510bf475ee
출처 데이터셋
uspto-grants-1985_10
특허 번호
US04544759

반응 노트

불러오는 중…