Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 4-Methoxycinnamate methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 4-Methoxy cinnamic acid | HCID 13245 | — |
| 생성물 | 4-Methoxycinnamate methyl ester | HCID 92841 | — |
반응 단계
A suspension of 300 g of 4-methoxycinnamic acid (J. Chem. Soc., Chem. Comm., 355, (1978)) and 25 ml of concentrated sulfuric acid in 1.7 liters of methanol is heated to reflux for 96 hours. The solution is concentrated, cooled, and filtered to give as a white solid, 4-methoxycinnamic acid methyl ester, mp 85°-86° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04548947 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-cde8d7e643394330bc4208001dec3e3b |
| 출처 메모 | uspto-grants-1985_10 |