Acetic Acid → gamma-Phenyl-gamma-butyrolactone

HRID 46742

반응식

HRID 46742 반응식
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9]([OH:12])(=[O:11])[CH3:10]>>[C:3]1([CH:2]2[O:12][C:9](=[O:11])[CH2:10][CH2:1]2)[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

참가 물질

3

반응 조건

온도
110 °C

실험 절차

Styrene in the amount of 20 grams was dissolved in 100 milliliters of acetic acid containing 10% potassium acetate. Ceric acetate in the amount of 0.005 mole was added and the reaction mixture was heated in a sealed tube at 110° C. overnight. The lactone, gamma-phenyl butyrolactone, was obtained in 70% yield.

출처 및 근거

ORD 기록
ord-3382055977444d27a94c974baede3424
출처 데이터셋
uspto-grants-1979_11
특허 번호
US04175089

연결된 노트

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