Acetic Anhydride → 1-Chloro-4-acetoxynonane

HRID 46961노트

반응식

HRID 46961 반응식
[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([OH:11])[CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:12](OC(=O)C)(=[O:14])[CH3:13]>>[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([O:11][C:12](=[O:14])[CH3:13])[CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

참가 물질

3

반응물 2

HCID 7918Acetic AnhydrideHCID 203860821-Chlorononan-4-ol

생성물 1

HCID 131047161-Chloro-4-acetoxynonane

실험 절차

A mixture of 1-chloro-4-nonanol (111.99 g.; 0.627 mole) and acetic anhydride (128.0 g.; 1.254 moles) is heated on a steam bath for 11/2 hours.

후처리

  1. temperatureis heated on a steam bath for 11/2 hours

출처 및 근거

ORD 기록
ord-87d8d09ce5804668a7dad94490cd33e9
출처 데이터셋
uspto-grants-1979_11
특허 번호
US04175203

반응 노트

불러오는 중…