반응식
[CH3:1][C:2]1[C:7]([C:8]#[N:9])=[CH:6][CH:5]=[CH:4][N:3]=1.[CH3:10][N:11]([CH:13]=O)[CH3:12]>>[CH3:10][N:11]([CH3:13])[CH:12]=[CH:1][C:2]1[C:7]([C:8]#[N:9])=[CH:6][CH:5]=[CH:4][N:3]=1참가 물질
3
실험 절차
N,N-dimethyl-2-(3-cyano-2-pyridyl)ethenamine was prepared using the procedure of 4 A from 2-methyl-3-cyanopyridine (9.0 g, 0.076 m), DMF acetal (11.0 g, 0.092 m) and DMF (50 mL) yielding N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine b.p.=133°-135° (0.3 mm), m.p.=49°-50° after sublimation at 50° (0.3 mm).
후처리
- customN,N-dimethyl-2-(3-cyano-2-pyridyl)ethenamine was prepared
출처 및 근거
- ORD 기록
- ord-4a2635ef6c464657ae9922b89defc428
- 출처 데이터셋
- uspto-grants-1979_11
- 특허 번호
- US04176183
연결된 노트
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