Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Dimethyl-tert-butylsilyl)oxybutan-1-ol → 2-(4-(Tert-butyldimethylsilyloxy)butoxy)-6-nitrobenzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Dimethyl-tert-butylsilyl)oxybutan-1-ol | HCID 186403 | — |
| 반응물 | Dinitrobenzonitrile | HCID 520718 | — |
| 생성물 | 2-(4-(Tert-butyldimethylsilyloxy)butoxy)-6-nitrobenzonitrile | HCID 66747043 | 25% |
반응 단계
Prepared as in Example 215c from 4-(tert-butyldimethyl-silyloxy)butan-1-ol and 2,6-dinitrobenzonitrile in 25% yield as a pale yellow solid. 1H NMR (400 MHz, DMSO-d6) δ 0.01 (s, 6H), 0.81-0.83 (m, 9H), 1.61-1.66 (m, 2H), 1.76-1.81 (m, 2H), 3.63 (t, J=6.8 Hz, 2H), 4.26 (t, J=6.4 Hz, 2H), 7.68-7.70 (m, 1H), 7.84-7.89 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08633186B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-0d4f0343312448b29bcb534ebe11d334 |
| 출처 메모 | uspto-grants-2014_01 |