Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 475208생성일: 2026년 10월 25일
2-(1-(tetrahydro-2H-pyran-2-yl)-1H-benzo[d]imidazol-5-yl)propan-2-amine → HCID 178456847, 화합물
https://huagongshe.com/reaction/475208
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-(1-(tetrahydro-2H-pyran-2-yl)-1H-benzo[d]imidazol-5-yl)propan-2-amine | HCID 71272671 | — |
| 반응물 | HCID 178478345 | HCID 178478345 | — |
| 생성물 | HCID 178456847 | HCID 178456847 | — |
반응 단계
A neat mixture of 94 (691 mg, 2.67 mmol) and 53 (210 mg, 0.89 mmol) was stirred under nitrogen at 140° C. for 18 h. The dark brown mixture was cooled to RT and was purified by preparative HPLC to afford 25 mg (7.5%) of I-17 as white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08637537B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_01 |
|---|
| ORD ID | ord-e4d49a00a1074bd1aacd2d18c6ee466c |
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| 출처 메모 | uspto-grants-2014_01 |
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