Ammonia → N,N-Diethylaniline

HRID 476305

반응식

HRID 476305 반응식
[NH3:1].[BH3:2].[CH2:3]([N:5]([CH2:12][CH3:13])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[CH3:4].B.[C:15]1([N:21]2[CH2:26][CH2:25][O:24][CH2:23][CH2:22]2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.B.[N:28]1[C:33]([CH3:34])=[CH:32][CH:31]=[CH:30][C:29]=1[CH3:35]>>[CH3:13][CH2:12][N:5]([C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][CH:11]=1)[CH2:3][CH3:4].[C:15]1([N:21]2[CH2:26][CH2:25][O:24][CH2:23][CH2:22]2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[N:28]1[C:33]([CH3:34])=[CH:32][CH:31]=[CH:30][C:29]=1[CH3:35].[NH3:1].[BH3:2]

참가 물질

8

반응물 4

HCID 222Ammonia2회HCID 83312Diethylaniline-boraneHCID 15265529(T-4)-Trihydro(4-phenylmorpholine-kappaN4)boronHCID 178419164HCID 178419164, 화합물

생성물 4

HCID 7061N,N-DiethylanilineHCID 79372,6-LutidineHCID 623394-PhenylmorpholineHCID 419330Ammonia;borane

실험 절차

For example, dimethylaniline borane can be reacted with ammonia to produce ammonia borane as shown below. (C6H5)(CH3)2N.BH3+NH3═(C6H5)(CH3)2N+NH3.BH3 In other examples, diethylaniline borane, phenylmorpholine borane or lutidine borane can be reacted with ammonia to form diethylaniline and ammonia borane, phenylmorpholine and ammonia borane, or lutidine and ammonia borane.

출처 및 근거

ORD 기록
ord-0a3d2fda4d6b4e7f9b7c1dc15d2c5642
출처 데이터셋
uspto-grants-2014_01
특허 번호
US08637703B2

연결된 노트

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