Formamide → HCID 21250683, 화합물

반응식

S(O)(O)(=O)=O.[NH2:6][C:7]1[N:8]=[C:9]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=2[O:21][CH2:22][CH3:23])[NH:10][C:11](=[O:14])[C:12]=1[NH2:13].[CH:24](N)=O>>[CH2:22]([O:21][C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][C:15]=1[C:9]1[N:8]=[C:7]2[C:12](=[N:13][CH:24]=[N:6]2)[C:11](=[O:14])[N:10]=1)[CH3:23]

참가 물질

반응물 2

HCID 713Formamide

HCID 136364570HCID 136364570, 화합물

생성물 1

HCID 21250683HCID 21250683, 화합물

실험 절차

In a similar manner to Example 1 reaction of 4,5-diamino-2-(2-ethoxyphenyl)pyrimidin-6-one sulphate (1.5 g) with formamide (15 ml) afforded the title compound, 0.36 g, m.p. 276°-277° C., (recrystallised from ethanol).

후처리

customafforded
customthe title compound, 0.36 g, m.p. 276°-277° C., (recrystallised from ethanol)

출처 및 근거

ORD 기록: ord-6a8a5cff74084cc6bef169f44834483f
출처 데이터셋: uspto-grants-1989_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04885301

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