Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methyl-3-oxopentanal → 2-Benzylthio-2-benzylthio-5-isopropyl-1,2,4-triazolo[1,5-a]pyrimidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methyl-3-oxopentanal | HCID 14786268 | — |
| 반응물 | HCID 178509291 | HCID 178509291 | — |
| 생성물 | 2-Benzylthio-2-benzylthio-5-isopropyl-1,2,4-triazolo[1,5-a]pyrimidine | HCID 19837373 | 96% |
반응 단계
This material was prepared in 96% yield from 3-amino-5-benzylthio-1,2,4-triazole and 4-methyl-3-oxopentanal following the general procedure described in Example 7. The desired product was isolated as a solid, m.p. 65°-66° C. IR and 1H NMR were in agreement with the assigned structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04886883 |
| 출처 데이터셋 | uspto-grants-1989_12 |
| ORD ID | ord-22ff46e77d9043b5808adaebdf58274d |
| 출처 메모 | uspto-grants-1989_12 |