Hydrochloric Acid → HCID 19835681, 화합물
반응식
[CH3:1][O:2][CH2:3][O:4][C:5]1[CH:12]=[CH:11][CH:10]=[C:9]([O:13][CH2:14][O:15][CH3:16])[C:6]=1[CH2:7][NH2:8].[ClH:17]>C(OCC)C>[ClH:17].[CH3:16][O:15][CH2:14][O:13][C:9]1[CH:10]=[CH:11][CH:12]=[C:5]([O:4][CH2:3][O:2][CH3:1])[C:6]=1[CH2:7][NH2:8]참가 물질
4
실험 절차
1.09 g of 2,6-bis(methoxymethoxy)benzylamine in 60 ml of anhydrous ethyl ether are treated with 1.92 ml of a 2.25 M solution of hydrogen chloride in anhydrous ethyl ether. A white solid precipitates which after filtering and carefully washing with anhydrous ethyl ether gives 2,6-bis(methoxymethoxy)benzylamine hydrochloride with melting point 151,5°-152° C.; the yield obtained is 95%. I.R. (KBr) 2580 cm-1 (NH3+), 1252 cm-1 (aromatic C--O), 1076 cm-1 (acetalic C--O), 773 cm-1 (phenyl).
후처리
- customA white solid precipitates which
- filtrationafter filtering
- washcarefully washing with anhydrous ethyl ether
출처 및 근거
- ORD 기록
- ord-a1b5b5e2946c44dd982f8784d26783bf
- 출처 데이터셋
- uspto-grants-1989_12
- 특허 번호
- US04888283
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