HCID 22064513, 화합물 → 498546-32-0

HRID 478688노트

반응식

HRID 478688 반응식
C([NH:4][C:5]1[C:6]([C:18]([OH:20])=[O:19])=[CH:7][C:8]2[C:13]([C:14]=1[N+:15]([O-:17])=[O:16])=[CH:12][CH:11]=[CH:10][CH:9]=2)(=O)C>Cl>[NH2:4][C:5]1[C:6]([C:18]([OH:20])=[O:19])=[CH:7][C:8]2[C:13]([C:14]=1[N+:15]([O-:17])=[O:16])=[CH:12][CH:11]=[CH:10][CH:9]=2

참가 물질

3

반응물 1

HCID 22064513HCID 22064513, 화합물

생성물 1

HCID 22064531498546-32-0

시약·촉매·용매 1

HCID 313Hydrochloric Acid용매

실험 절차

A solution of 1 g of the compound obtained in Step 1 in 18 ml of hydrochloric acid is refluxed for 4 hours and then poured onto ice. The precipitate formed is filtered off, washed with water until the pH is 5-6 and then dried, allowing the expected product to be isolated.

후처리

  1. additionpoured onto ice
  2. customThe precipitate formed
  3. filtrationis filtered off
  4. washwashed with water until the pH is 5-6
  5. customdried
  6. customto be isolated

출처 및 근거

ORD 기록
ord-087c1d3dd4404494aaac4f4b2d48a6b6
출처 데이터셋
uspto-grants-2003_11
특허 번호
US06642248B2

반응 노트

불러오는 중…