4-Fluoroaniline → HCID 9857738, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[CH:8]/[S:9](Cl)(=[O:11])=[O:10])=[CH:5][CH:4]=1.[F:15][C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1>>[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[CH:8]/[S:9]([NH:20][C:19]2[CH:21]=[CH:22][C:16]([F:15])=[CH:17][CH:18]=2)(=[O:11])=[O:10])=[CH:5][CH:4]=1

참가 물질

반응물 2

HCID 97314-Fluoroaniline

HCID 12114473HCID 12114473, 화합물

생성물 1

HCID 9857738HCID 9857738, 화합물수율 86.4%

실험 절차

A solution of (E)-4-methoxystyrylsulfonyl chloride (10 mmol) and 4-fluoroaniline (10 mmol) was subjected to General Procedure 1, part B. The title compound, melting point 115-117° C., was obtained 86.4% yield.

출처 및 근거

ORD 기록: ord-230b64d4dcd345869f4626e658e91b74
출처 데이터셋: uspto-grants-2003_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06646009B2

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