Phosphorus pentachloride → HCID 18766652, 화합물

HRID 480929노트

반응식

HRID 480929 반응식
[Na+].[C:2]([C:4]1[CH:9]=[CH:8][C:7]([NH:10][S:11](=O)(=[O:13])[O-:12])=[C:6]([O:15][CH3:16])[CH:5]=1)#[N:3].P(Cl)(Cl)(Cl)(Cl)[Cl:18]>O=P(Cl)(Cl)Cl>[C:2]([C:4]1[CH:9]=[CH:8][C:7]([NH:10][S:11]([Cl:18])(=[O:13])=[O:12])=[C:6]([O:15][CH3:16])[CH:5]=1)#[N:3]

참가 물질

4

반응물 2

HCID 24819Phosphorus pentachlorideHCID 69677029HCID 69677029, 화합물

생성물 1

HCID 18766652HCID 18766652, 화합물

시약·촉매·용매 1

HCID 24813Phosphorus oxychloride용매

실험 절차

To a soultion of N-(4-cyano-2-methoxyphenyl)-sulfamic acid sodium salt (1 mmol) at 0° C. in POCl3 (1 mL) is added phosphorous pentachloride (1.2 mmol). Upon reaction completion, the reaction mixture is concentrated and the crude material will be carried onto the next step without further purification.

후처리

  1. customUpon reaction completion
  2. concentrationthe reaction mixture is concentrated
  3. customthe crude material will be carried onto the next step without further purification

출처 및 근거

ORD 기록
ord-ff7dd18215fc43dbb282092208acdd36
출처 데이터셋
uspto-grants-2003_11
특허 번호
US06653347B2

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