Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrahydrofuran → Methyl 2-(2-formyl-4-ethylphenoxy)propionate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrahydrofuran | HCID 8028 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Methyl 2-bromopropionate | HCID 95576 | — |
| 반응물 | 4-Ethyl-2-hydroxybenzaldehyde | HCID 10236017 | — |
| 생성물 | Methyl 2-(2-formyl-4-ethylphenoxy)propionate | HCID 18981013 | — |
반응 단계
By the method of Example 1, Step F, 32.33 grams (0.215 mole) of 4-ethylsalicylaldehyde and 35.9 grams (0.215 mole) of methyl 2-bromopropionate was reacted in the presence of 35.7 grams (0.258 mole) of potassium carbonate in 50 mL of tetrahydrofuran, yielding 49.16 grams of methyl 2-(2-formyl-4-ethylphenoxy)propionate. The NMR spectrum was consistent with the proposed spectrum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05798316 |
| 출처 데이터셋 | uspto-grants-1998_08 |
| ORD ID | ord-a38643e302ce4e87917a8e37b9e017fe |
| 출처 메모 | uspto-grants-1998_08 |