Acetic Anhydride → HCID 15157701, 화합물

HRID 483777노트

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HRID 483777 반응식
[OH:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][CH:6]=[C:5]2[CH:11]1[CH:16]2[CH2:17][CH2:18][N:13]([CH2:14][CH2:15]2)[CH2:12]1.[C:19](OC(=O)C)(=[O:21])[CH3:20]>N1C=CC=CC=1>[C:19]([O:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][CH:6]=[C:5]2[CH:11]1[CH:16]2[CH2:17][CH2:18][N:13]([CH2:14][CH2:15]2)[CH2:12]1)(=[O:21])[CH3:20]

참가 물질

4

반응물 2

HCID 7918Acetic AnhydrideHCID 98346891H-Indol-5-ol, 3-(1-azabicyclo[2.2.2]oct-3-yl)-

생성물 1

HCID 15157701HCID 15157701, 화합물

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

200 mg of 3-(5-hydroxy-3-indolyl)quinuclidine are dissolved in 10 ml of pyridine and 5 ml of acetic anhydride are added with cooling. After one hour, the mixture is worked up as is customary. 3-(5-acetoxy-3-indolyl)quinuclidine is obtained.

후처리

  1. temperaturewith cooling

출처 및 근거

ORD 기록
ord-f31d5a51df67437d94123c2a9c687454
출처 데이터셋
uspto-grants-1993_07
특허 번호
US05227386

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