2,6-Dimethyl-4-nitroaniline → 2-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline

HRID 484787

반응식

HRID 484787 반응식
Cl[C:2]1[CH2:6][CH2:5][CH2:4][N:3]=1.[CH3:7][C:8]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[C:11]([CH3:18])[C:9]=1[NH2:10]>>[CH3:7][C:8]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[C:11]([CH3:18])[C:9]=1[NH:10][C:2]1[CH2:6][CH2:5][CH2:4][N:3]=1

참가 물질

3

반응물 2

HCID 281592,6-Dimethyl-4-nitroanilineHCID 135201412-Chloro-1-pyrroline

생성물 1

HCID 202723942-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline

실험 절차

A mixture of 2-chloro-1-pyrroline, prepared as in Example 1, and 19.9 g (0.12 mole) of the aniline product of Example 6 were heated at reflux overnight, according to the general method of Example 8. The title compound was isolated and used for subsequent reactions without further purification. Structure assignment was supported by nmr and infrared spectra.

후처리

  1. temperaturewere heated
  2. temperatureat reflux overnight

출처 및 근거

ORD 기록
ord-b73808b27f264206b52ae5c5d7b1945f
출처 데이터셋
uspto-grants-1985_08
특허 번호
US04533739

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