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Hydrochloric Acid → HCID 20272264, 화합물

HRID 484897
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HRID 484897 반응식
[CH2:1]([N:3]([CH2:27][CH3:28])[CH2:4][CH2:5][CH2:6][N:7]1[C:15]2[C:10](=[CH:11][C:12]([NH2:17])=[CH:13][C:14]=2[NH2:16])[C:9]([NH:18][CH2:19][CH2:20][CH2:21][N:22]([CH2:25][CH3:26])[CH2:23][CH3:24])=[N:8]1)[CH3:2].[ClH:29].C(OCC)C>C(O)C>[ClH:29].[ClH:29].[ClH:29].[ClH:29].[CH2:27]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][CH2:6][N:7]1[C:15]2[C:10](=[CH:11][C:12]([NH2:17])=[CH:13][C:14]=2[NH2:16])[C:9]([NH:18][CH2:19][CH2:20][CH2:21][N:22]([CH2:23][CH3:24])[CH2:25][CH3:26])=[N:8]1)[CH3:28]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 20135876HCID 20135876, 화합물

생성물 1

HCID 20272264HCID 20272264, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

In 20 ml of absolute ethyl alcohol was dissolved 2.5 g of the 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)-5,7-diaminoindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)-5,7-diaminoindazole tetrahydrochloride having the following analytical value.

후처리

  1. temperatureunder cooling with ice
  2. customto separate crystals
  3. customThe crystals were obtained by filtration
  4. customdried

출처 및 근거

ORD 기록
ord-1a3fecb9c512447e97256b92bc96ba6b
출처 데이터셋
uspto-grants-1985_08
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04533731

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