Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Decanethiol → HCID 178443464, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Decanethiol | HCID 8917 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | HCID 178524541 | HCID 178524541 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 178443464 | HCID 178443464 | — |
반응 단계
2 g (6.08 millimols) of tetrachlorophthalic acid N-2-hydroxyethylimide, 5.30 g (30.4 millimols) of n-decanethiol, 6.30 g (45.6 millimols) of potassium carbonate and 20 ml of N,N-dimethylformamide are stirred at 25° C. for 7 hours. The mixture is acidified and extracted with methylene chloride. After recrystallisation from n-hexane at 0° C., 3.75 g (70% of theory) of the title compound are obtained; melting point 57°-8° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04537977 |
| 출처 데이터셋 | uspto-grants-1985_08 |
| ORD ID | ord-f1d9b95f187446bcaa47845f35563cf3 |
| 출처 메모 | uspto-grants-1985_08 |