Pyridine → 1-(2-Ethoxy-2-oxoethyl)pyridin-1-ium chloride

HRID 487342노트

반응식

HRID 487342 반응식
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:7][CH2:8][C:9]([O:11][CH2:12][CH3:13])=[O:10]>C(OCC)(=O)C>[Cl-:7].[CH2:12]([O:11][C:9]([CH2:8][N+:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)=[O:10])[CH3:13]

참가 물질

4

반응물 2

HCID 1049PyridineHCID 7751Ethyl chloroacetate

생성물 1

HCID 111381401-(2-Ethoxy-2-oxoethyl)pyridin-1-ium chloride

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

Pyridine (1 equivalent) and ethyl chloroacetate (1 equivalent) in ethyl acetate were heated (70° C.) for 24 hours. The reaction mixture was cooled to room temperature and the resulting crystalline pyridinium salt filtered, washed with ethyl acetate, and dried in vacuum.

후처리

  1. filtrationthe resulting crystalline pyridinium salt filtered
  2. washwashed with ethyl acetate
  3. customdried in vacuum

출처 및 근거

ORD 기록
ord-b15aed9988544fb3aa12a2a2f218286b
출처 데이터셋
uspto-grants-1994_03
특허 번호
US05294721

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