Hydrochloric Acid → HCID 178454908, 화합물

HRID 488185노트

반응식

HRID 488185 반응식
[CH2:1]([O:3][CH:4]([PH:8](=[O:12])OCC)[O:5][CH2:6][CH3:7])[CH3:2].[CH2:13]([Li])[CH2:14][CH2:15][CH3:16].Cl>CCCCCC>[CH2:13]([PH:8](=[O:12])[CH:4]([O:3][CH2:1][CH3:2])[O:5][CH2:6][CH3:7])[CH2:14][CH2:15][CH3:16]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 178418339ButyllithiumHCID 178472284HCID 178472284, 화합물

생성물 1

HCID 178454908HCID 178454908, 화합물

시약·촉매·용매 1

HCID 8058Hexane용매

실험 절차

Following the procedure of Example 8, but using 1.96 g of ethyl diethoxymethylphosphinate and 12.5 ml of a 1.6 molar solution of n-butyl lithium in n-hexane and adding 20 ml of 0.1M hydrochloric acid prior to extraction, n-butyl(diethoxymethyl) phosphine oxide is obtained as a colourless oil.

후처리

  1. extractionto extraction

출처 및 근거

ORD 기록
ord-2277432bade34b168962db8a9fb747e3
출처 데이터셋
uspto-grants-1994_03
특허 번호
US05298663

반응 노트

불러오는 중…