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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 491437생성일: 2026년 10월 26일

Methanesulfonyl chloride → (4aS,8aR)-4-(3,4-Diethoxyphenyl)-2-(1-methanesulfonyl-piperidin-4-yl)-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one

https://huagongshe.com/reaction/491437

반응식

참여 물질

역할이름HCID투입량
반응물Methanesulfonyl chlorideHCID 31297—
반응물(4aS,8aR)-4-(3,4-Diethoxyphenyl)-2-[1-(toluene-4-sulfonyl)-piperidin-4-yl]-4a,5,8,8a-tetrahydro-2H-phthalazin-1-oneHCID 10175016—
생성물(4aS,8aR)-4-(3,4-Diethoxyphenyl)-2-(1-methanesulfonyl-piperidin-4-yl)-4a,5,8,8a-tetrahydro-2H-phthalazin-1-oneHCID 10310924—

반응 단계

Prepared from methanesulfonylchloride and starting compound A2 as described for compound 1. Crystallisation from methanol/water. M.p. 99-102° C.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07531540B2
출처 데이터셋uspto-grants-2009_05
ORD IDord-d37e4281f2e9484094012e1f14c5b2d0
출처 메모uspto-grants-2009_05