Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrahydrothiophene → Phenacyltetrahydrothiophenium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrahydrothiophene | HCID 1127 | — |
| 반응물 | Phenacyl bromide | HCID 6259 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | Phenacyltetrahydrothiophenium bromide | HCID 11346720 | — |
반응 단계
150 Parts of 2-bromoacetophenone was dissolved in 375 parts of acetone, and 66.5 parts of tetrahydrothiophene was added dropwise thereto. After the mixture was stirred at room temperature for 24 hours, white solid obtained was filtered, washed with acetone and then dried to obtain 207.9 parts of 1-(2-oxo-2-phenylethyl)tetrahydrothiophenium bromide in the form of white crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07531686B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-37e02a890daa4cc6978efe183bf6854a |
| 출처 메모 | uspto-grants-2009_05 |