HRID492267

反应详情

EQUATION

反应方程式

HRID 492267 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

150 Parts of 2-bromoacetophenone was dissolved in 375 parts of acetone, and 66.5 parts of tetrahydrothiophene was added dropwise thereto. After the mixture was stirred at room temperature for 24 hours, white solid obtained was filtered, washed with acetone and then dried to obtain 207.9 parts of 1-(2-oxo-2-phenylethyl)tetrahydrothiophenium bromide in the form of white crystals.

WORKUP

后处理

  1. additionwas added dropwise
  2. customwhite solid obtained
  3. filtrationwas filtered
  4. washwashed with acetone
  5. customdried