N-(2-nitro-4-trifluoromethylsulfonyl-phenyl)-acetamide → 2-Nitro-4-(trifluoromethanesulfonyl)aniline
반응식
[N+:1]([C:4]1[CH:9]=[C:8]([S:10]([C:13]([F:16])([F:15])[F:14])(=[O:12])=[O:11])[CH:7]=[CH:6][C:5]=1[NH:17]C(=O)C)([O-:3])=[O:2]>Cl.O>[N+:1]([C:4]1[CH:9]=[C:8]([S:10]([C:13]([F:16])([F:14])[F:15])(=[O:11])=[O:12])[CH:7]=[CH:6][C:5]=1[NH2:17])([O-:3])=[O:2]참가 물질
4
실험 절차
Reflux N-(2-nitro-4-trifluoromethylsulfonyl-phenyl)-acetamide (600 mg) for 40 minutes in concentrated HCl (15 mL) and water (5 mL). Cool the mixture to room temperature and collect the precipitate obtain 2-nitro-4-trifluoromethylsulfonyl-phenylamine. D. 4-Trifluoromethylsulfonyl-benzene-1,2-diamine
후처리
- customcollect the precipitate
출처 및 근거
- ORD 기록
- ord-b3f5690884f442e4970001d0a724d8cb
- 출처 데이터셋
- uspto-grants-2005_09
- 특허 번호
- US06943199B2
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