2,5-Dimethoxytetrahydrofuran → HCID 22317392, 화합물

HRID 498187노트

반응식

HRID 498187 반응식
[N+:1]([C:4]1[CH:9]=[C:8]([NH2:10])[CH:7]=[CH:6][C:5]=1[NH2:11])([O-:3])=[O:2].CO[CH:14]1[CH2:18][CH2:17][CH:16](OC)O1>CC(O)=O>[N+:1]([C:4]1[CH:9]=[C:8]([N:10]2[CH:14]=[CH:18][CH:17]=[CH:16]2)[CH:7]=[CH:6][C:5]=1[NH2:11])([O-:3])=[O:2]

참가 물질

4

반응물 2

HCID 790982,5-DimethoxytetrahydrofuranHCID 43383702-Nitro-4-phenylenediamine

생성물 1

HCID 22317392HCID 22317392, 화합물

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

The title compound was prepared from 2-nitro-1,4-phenylenediamine [CAS-No. 5307-14-2] (20 g, 131 mmol) and 2,5-dimethoxytetrahydrofuran (18.3 mL, 135 mmol) in HOAc (37 mL) at 95° C. for 3 h according to the general procedure F. Obtained as a red solid (13.5 g).

출처 및 근거

ORD 기록
ord-ad337e410b654db2b6432bc140bfd210
출처 데이터셋
uspto-grants-2005_09
특허 번호
US06949542B2

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