Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2-Nitro-4-trifluoromethoxy-phenyl)-carbamic acid tert-butyl ester → Carbamic acid,[2-amino-4-(trifluoromethoxy)phenyl]-,1,1-dimethylethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2-Nitro-4-trifluoromethoxy-phenyl)-carbamic acid tert-butyl ester | HCID 69489589 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | Carbamic acid,[2-amino-4-(trifluoromethoxy)phenyl]-,1,1-dimethylethyl ester | HCID 69489489 | — |
반응 단계
The title compound was prepared from (2-nitro-4-trifluoromethoxy-phenyl)-carbamic acid tert-butyl ester (Example A22) (10.38 g, 32.2 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a light brown solid (8.76 g, 93%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06949542B2 |
| 출처 데이터셋 | uspto-grants-2005_09 |
| ORD ID | ord-2fac2924806b4032976ad77bf9f8f930 |
| 출처 메모 | uspto-grants-2005_09 |