Hydrochloric Acid → 2-Aminoquinoline-6-carboxylic Acid Hydrochloride

반응식

[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:12]([O:14]CC)=[O:13])[CH:8]=2)[N:3]=1.[ClH:17]>>[ClH:17].[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:12]([OH:14])=[O:13])[CH:8]=2)[N:3]=1

참가 물질

반응물 2

HCID 313Hydrochloric Acid

HCID 17834348Ethyl 2-aminoquinoline-6-carboxylate

생성물 1

HCID 691425542-Aminoquinoline-6-carboxylic Acid Hydrochloride

실험 절차

330 mg of ethyl 2-aminoquinoline-6-carboxylate was stirred in 30 ml of 6 M hydrochloric acid at 80° C. overnight. The solvent was evaporated, and the residue was washed with ethyl acetate to obtain the title compound.

후처리

customThe solvent was evaporated
washthe residue was washed with ethyl acetate

출처 및 근거

ORD 기록: ord-433f363192db47b18bcac0f46394763f
출처 데이터셋: uspto-grants-2004_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06710056B2

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