Sulfuric Acid → Urea sulfate

HRID 51978

반응식

HRID 51978 반응식
[NH2:1][C:2]([NH2:4])=[O:3].[S:5](=[O:9])(=[O:8])([OH:7])[OH:6].[OH-].[Na+]>O>[S:5](=[O:7])(=[O:6])([OH:9])[OH:8].[NH2:1][C:2]([NH2:4])=[O:3]

참가 물질

5

반응물 3

HCID 1118Sulfuric AcidHCID 1176UreaHCID 14798Sodium Hydroxide

생성물 1

HCID 159909Urea sulfate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Prilled urea (17.5 grams, 0.29 moles) was dissolved in 53.5 grams water. To this solution was slowly added sulfuric acid (29.0 grams, 0.26 moles, 89.3%) at 66° C. The temperature was maintained below 50° C. in a cooling bath during the addition. The final solution on titration with 0.5 N NaOH (phenolphthalein indicator) was 5.3 N, which is equal to the theoretical value.

후처리

  1. customat 66° C
  2. temperatureThe temperature was maintained below 50° C. in a cooling bath during the addition

출처 및 근거

ORD 기록
ord-93142238973f4f45b4e085e5586d9314
출처 데이터셋
uspto-grants-1997_04
특허 번호
US05616151

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