Benzoyl chloride → HCID 19963672, 화합물

HRID 52437노트

반응식

HRID 52437 반응식
[CH2:1]([CH2:7][C:8]([NH2:10])=[S:9])[C:2]1[O:6][CH:5]=[CH:4][CH:3]=1.[C:11](Cl)(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(OCC)(=O)C>N1C=CC=CC=1>[C:11]([NH:10][C:8](=[S:9])[CH2:7][CH2:1][C:2]1[O:6][CH:5]=[CH:4][CH:3]=1)(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

참가 물질

5

반응물 3

HCID 7412Benzoyl chlorideHCID 8857Ethyl AcetateHCID 199636792-Furfurylthioacetamide

생성물 1

HCID 19963672HCID 19963672, 화합물

시약·촉매·용매 1

HCID 1049Pyridine용매

반응 조건

온도
60 °C

실험 절차

12.11 g (0.07 mol) of 2-furfurylthioacetamide was dissolved in 30 ml of pyridine. To the above solution, 9.94 g (0.07 mol) of benzoylchloride was added, and the mixture was stirred at 60° C. for 15 hours. The solvent was distilled away from the reaction mixture, and a residue thus obtained was added to ethyl acetate and washed successively with water twice, 1N hydrochloric acid, water three times, and brine. A resultant organic extract layer was dried, and the solvent was distilled away therefrom.

후처리

  1. distillationThe solvent was distilled away from the reaction mixture
  2. customa residue thus obtained
  3. washwashed successively with water twice
  4. customA resultant organic extract layer was dried
  5. distillationthe solvent was distilled away

출처 및 근거

ORD 기록
ord-8daf3d01e7a4411b93e67d7293813538
출처 데이터셋
uspto-grants-1997_04
특허 번호
US05616711

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