Benzylamine → HCID 118201132, 화합물
반응식
[CH2:1]([NH2:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:9]1([CH2:13][CH:14]=O)[CH2:12][CH2:11][CH2:10]1>C(Cl)Cl>[CH:9]1([CH2:13][CH:14]=[N:8][CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH2:12][CH2:11][CH2:10]1참가 물질
4
실험 절차
Benzylamine (2.95 g, 27.5 mmol) was added to a mixture of cyclobutylacetaldehyde (30.6 mmol) in CH2Cl2 (˜238 mL) and molecular sieves (5.0 g) and the mixture was stirred at room temperature for 5.5 hours. The mixture was filtered over Celite and the solvent was removed under vacuum to yield 5.45 g of crude N-(2-cyclobutylethylidene)-1-phenylmethanamine.
후처리
- filtrationThe mixture was filtered over Celite
- customthe solvent was removed under vacuum
출처 및 근거
- ORD 기록
- ord-68fd615743254ce5821775dd2ee41d1b
- 출처 데이터셋
- uspto-grants-2016_05
- 특허 번호
- US09346853B2
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