Hydrochloric Acid → HCID 178418457, 화합물

HRID 53612

반응식

HRID 53612 반응식
[C:1]([C:4]1[CH:5]=[C:6]([CH:8]=[C:9]([C:11](=[O:13])[CH3:12])[CH:10]=1)[NH2:7])(=[O:3])[CH3:2].[C:14]([NH:16][C:17]([NH2:19])=[NH:18])#[N:15].[ClH:20]>O>[ClH:20].[C:1]([C:4]1[CH:5]=[C:6]([NH:7][C:14]([NH:16][C:17]([NH2:19])=[NH:18])=[NH:15])[CH:8]=[C:9]([C:11](=[O:13])[CH3:12])[CH:10]=1)(=[O:3])[CH3:2]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 463010Cni H1894HCID 178418324HCID 178418324, 화합물

생성물 1

HCID 178418457HCID 178418457, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Compound No. 12. A suspension of 3,5-diacetylaniline (0.531 g) in water (8 mL) was treated with cyanoguanidine (0.285 g) and conc. HCl (0.25 mL) and heated at reflux. After 6 hr the mixture was cooled and concentrated and 0.248 g of off-white solid was filtered out and dried to give N-(3,5-diacetylphenyl)biguanide hydrochloride, mp 260°-70° C. (dec).

후처리

  1. temperatureheated
  2. temperatureat reflux
  3. temperatureAfter 6 hr the mixture was cooled
  4. concentrationconcentrated
  5. filtration0.248 g of off-white solid was filtered out
  6. customdried

출처 및 근거

ORD 기록
ord-40633f04293e45b78cf81ea0df8fe2ac
출처 데이터셋
uspto-grants-1997_04
특허 번호
US05620983

연결된 노트

불러오는 중…