Sodium Hydroxide → HCID 178418584, 화합물

HRID 542315노트

반응식

HRID 542315 반응식
[NH2:1][CH2:2][CH:3]([C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][CH:9]=1)[CH2:4][P:5]([OH:7])[OH:6].[OH-].[Na+:16]>>[NH2:1][CH2:2][CH:3]([C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][CH:9]=1)[CH2:4][PH:5](=[O:6])[O-:7].[Na+:16]

참가 물질

3

반응물 2

HCID 14798Sodium HydroxideHCID 117761763-Amino-2-(4-chlorophenyl)propylphosphonous acid

생성물 1

HCID 178418584HCID 178418584, 화합물

실험 절차

A solution of 0.25 g of 3-amino-2-(4-chlorophenyl)propylphosphonous acid in 10 ml of 0.1M sodium hydroxide solution is stirred at room temperature for a period of 1 hour, and then concentrated under reduced pressure to give sodium 3-amino-2-(4-chlorophenyl)propylphosphinate as a hygroscopic solid, 31P=+26.0 ppm (D2O).

후처리

  1. concentrationconcentrated under reduced pressure

출처 및 근거

ORD 기록
ord-1bb85080faf64284ac007c12801e8fa9
출처 데이터셋
uspto-grants-1987_04
특허 번호
US04656298

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