HCID 13210257, 화합물 → HCID 10402160, 화합물

HRID 543375노트

반응식

HRID 543375 반응식
[Cl:1]CC([NH:5][CH2:6][C:7]1[CH:12]=[C:11]([C:13]([CH3:16])([CH3:15])[CH3:14])[CH:10]=[C:9]([S:17]([CH3:20])(=[O:19])=[O:18])[C:8]=1[OH:21])=O>Cl.C(O)C>[ClH:1].[NH2:5][CH2:6][C:7]1[CH:12]=[C:11]([C:13]([CH3:14])([CH3:15])[CH3:16])[CH:10]=[C:9]([S:17]([CH3:20])(=[O:18])=[O:19])[C:8]=1[OH:21]

참가 물질

4

반응물 1

HCID 13210257HCID 13210257, 화합물

생성물 1

HCID 10402160HCID 10402160, 화합물

시약·촉매·용매 2

HCID 313Hydrochloric Acid용매HCID 702Ethanol용매

실험 절차

6.3 g (0.028 mol) of 2-chloro-N-[5-(1,1-dimethylethyl)-2-hydroxy-3-methylsulfonylbenzyl]acetamide in a mixture of 20 ml of concentrated hydrochloric acid and 40 ml of ethanol are boiled under reflux for 16 hours. The precipitated product is filtered off with suction and recrystallized from ethanol.

후처리

  1. temperatureunder reflux for 16 hours
  2. filtrationThe precipitated product is filtered off with suction
  3. customrecrystallized from ethanol

출처 및 근거

ORD 기록
ord-0eec8b5262444e9e87f286f134e53400
출처 데이터셋
uspto-grants-1987_04
특허 번호
US04661636

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