Methyl iodide → HCID 178504040, 화합물

HRID 543794노트

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HRID 543794 반응식
[F:1][C:2]([F:9])([F:8])[CH2:3][NH:4][C:5]([NH2:7])=[S:6].[CH3:10][I:11]>CCO>[IH:11].[F:1][C:2]([F:9])([F:8])[CH2:3][NH:4][C:5](=[NH:7])[S:6][CH3:10]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 202028121-(2,2,2-Trifluoroethyl)thiourea

생성물 1

HCID 178504040HCID 178504040, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A solution of 2,2,2-trifluoroethylthiourea (8.0 g.) and methyl iodide (3.5 g.) in EtOH (40 ml.) was heated under reflux for 70 minutes, then evaporated to dryness in vacuo. The residue was triturated with ether to give 2,2,2-trifluoroethyl-S-methylisothiourea hydroiodide, m.p. 154°-156° (90%).

후처리

  1. temperatureunder reflux for 70 minutes
  2. customevaporated to dryness in vacuo
  3. customThe residue was triturated with ether

출처 및 근거

ORD 기록
ord-eb664b0dcd9f44d985ecb0985c5b3da2
출처 데이터셋
uspto-grants-1984_05
특허 번호
US04447441

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