Hydrochloric Acid → HCID 178479216, 화합물

HRID 543837노트

반응식

HRID 543837 반응식
C([NH:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)(=O)C.[ClH:14]>>[ClH:14].[NH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 178474793HCID 178474793, 화합물

생성물 1

HCID 178479216HCID 178479216, 화합물

실험 절차

A mixture of 1-(3-acetamidopropyl)-1H-tetrazole-5-thiol (85 g) and 6 N hydrochloric acid (1 l) was refluxed for 75 minutes under stirring. The reaction mixture was concentrated in vacuo and precipitates were collected by filtration and washed with hexane and diethyl ether to give 1-(3-aminopropyl)-1H-tetrazole-5-thiol hydrochloride (67.15 g).

후처리

  1. temperaturewas refluxed for 75 minutes
  2. concentrationThe reaction mixture was concentrated in vacuo
  3. customprecipitates
  4. filtrationwere collected by filtration
  5. washwashed with hexane and diethyl ether

출처 및 근거

ORD 기록
ord-6736eb8bdc694aa18722bcfb790dff69
출처 데이터셋
uspto-grants-1984_05
특허 번호
US04447429

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