Hydrochloric Acid → HCID 178458047, 화합물

반응식

C([NH:4][CH2:5][CH:6]([N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)[CH3:7])(=O)C.[ClH:14]>>[ClH:14].[NH2:4][CH2:5][CH:6]([N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)[CH3:7]

참가 물질

반응물 2

HCID 313Hydrochloric Acid

HCID 178474792HCID 178474792, 화합물

생성물 1

HCID 178458047HCID 178458047, 화합물

실험 절차

A mixture of 1-[1-(acetamidomethyl)ethyl]-1H-tetrazole-5-thiol (23 g) and 6 N aqueous hydrochloric acid (300 ml) was refluxed for 2 hours under stirring and evaporated to dryness. The residue was triturated with diethyl ether to give 1-[1-(aminomethyl)ethyl]-1H-tetrazole-5-thiol hydrochloride (19 g), mp 208° to 210° C.

후처리

temperaturewas refluxed for 2 hours
customevaporated to dryness
customThe residue was triturated with diethyl ether

출처 및 근거

ORD 기록: ord-77ea3384e3b94a37bbccab2e8e9d5580
출처 데이터셋: uspto-grants-1984_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04447429

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