참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Methyl 2-(4-hydroxyphenoxy)acetate | HCID 602731 | — |
| 용매 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | (4-Hydroxyphenoxy)acetic acid | HCID 15881 | — |
반응 단계
(4-Hydroxy-phenoxy)-acetic acid methyl ester 11 (20 grams, 109.89 mmol) is added to 10% sodium hydroxide solution (100 mL) and heated to 90° C. on water bath for 6 hours. The reaction mixture is cooled to room temperature, and the pH is adjusted to 2 with distilled HCl. Crude 12, is filtered, dried, and can be recrystallised in appropriate solvent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07935843B2 |
|---|
| 출처 데이터셋 | uspto-grants-2011_05 |
|---|
| ORD ID | ord-9b60dbd7e8564d3083558297cd3660ca |
|---|
| 출처 메모 | uspto-grants-2011_05 |
|---|
