tert-butyl N'-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylate → 5-Chloro-2-cyclohexyl-valeric acid hydrazide hydrochloride
반응식
[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([CH:17]1[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1)[C:6]([NH:8][NH:9]C(OC(C)(C)C)=O)=[O:7]>Cl.O1CCOCC1>[ClH:1].[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([CH:17]1[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1)[C:6]([NH:8][NH2:9])=[O:7]참가 물질
4
실험 절차
tert-Butyl N′-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylate (155 mg) was dissolved in a solution of 4 N hydrogen chloride in dioxane (2 ml), and the reaction solution was stirred at room temperature for one hour. The reaction solution was concentrated under reduced pressure to obtain 144 mg of the title compound. The property value of the compound is as follows.
후처리
- concentrationThe reaction solution was concentrated under reduced pressure
출처 및 근거
- ORD 기록
- ord-3003b35eed6748cfa68010ac9fd15804
- 출처 데이터셋
- uspto-grants-2011_05
- 특허 번호
- US07935815B2
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