Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Butanaminium, N,N,N-tributyl-, azide → Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Butanaminium, N,N,N-tributyl-, azide | HCID 5743232 | — |
| 반응물 | Ethanethioic acid cis-(+/-)-S-[tetrahydro-5-[[[(trifluoromethyl)-sulfonyl]oxy]methyl]-3-furanyl]ester | HCID 86750330 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester | HCID 86750331 | 87.8% |
반응 단계
The title compound is prepared by the procedure of Example 43 using 0.560 g of product from Example 60 in 2 ml of methylene chloride, 0.569 g of tetrabutylammonium azide in 2 ml of methylene chloride to give 0.321 g of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05623081 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-8808e9b3904943e3bfecb2393f2ea08f |
| 출처 메모 | uspto-grants-1997_04 |