HRID54778

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCCC[N+](CCCC)(CCCC)CCCC.[N-]=[N+]=[N-]

HCID5743232

1-Butanaminium, N,N,N-tributyl-, azide

C16H36N4

结构：CC(=O)S[C@@H]1CO[C@H](COS(=O)(=O)C(F)(F)F)C1

HCID86750330

未命名化合物

PRODUCTS

生成物

结构：CC(=O)S[C@@H]1CO[C@H](CN=[N+]=[N-])C1

HCID86750331

未命名化合物

收率 87.8%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

2 次

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 43 using 0.560 g of product from Example 60 in 2 ml of methylene chloride, 0.569 g of tetrabutylammonium azide in 2 ml of methylene chloride to give 0.321 g of the desired product.